Products & ReviewSeparations

DisQuE Quechers, AOAC Method Sample Preparation Kit, Pouches

DisQuE Dispersive Sample Preparation used for QUECHERS Method AOAC Method 2007.01. The kit consists of 100 units each of salt pouches, empty 50mL centrifuge tubes and clean-up tubes. Each DisQuE pouch contains 6 grams of magnesium sulphate and 1.5 grams of sodium acetate. Each 2 mL DisQuE Clean-Up tube contains 150 mg of magnesium sulphate and 50 mg PSA (primary-secondary amine SPE sorbent)

Waters

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Description

DisQuE Dispersive Sample Preparation used for QUECHERS Method AOAC Method 2007.01. The kit consists of 100 units each of salt pouches, empty 50mL centrifuge tubes and clean-up tubes. Each DisQuE pouch contains 6 grams of magnesium sulphate and 1.5 grams of sodium acetate. Each 2 mL DisQuE Clean-Up tube contains 150 mg of magnesium sulphate and 50 mg PSA (primary-secondary amine SPE sorbent)

Application NoteEnvironmental

Addressing the global challenge of PFAS contamination

Per- and polyfluoroalkyl substances (PFAS) are a class of synthetic chemicals that pose significant environmental and health challenges due to their persistence and bioaccumulation. PFAS testing is one of the most pressing issues facing analytical labs today. As global attention grows, so does the demand for reliable answers.

Technologies such as liquid chromatography-tandem mass spectrometry (LC-MS/ MS) and high-resolution mass spectrometry (HRMS) can be essential for assessing PFAS contamination accurately. Discover how advanced LC-MS/MS and HRMS technologies are helping scientists and regulators tackle PFAS challenges head-on.

From sample preparation to data analysis, explore how Waters Corporation provides the tools needed to measure, manage, and mitigate the impact of PFAS, driving scientific progress and regulatory compliance.


Application NoteSeparations

Oasis PRiME HLB Cartridges and DisQuE QuEChERS Products for UPLC-MS/MS Mycotoxin Analysis in Cereal Grains

Ingestion of food containing only parts-per-billion (µg/kg) concentration of some mycotoxins may cause severe illness. Therefore, sensitive and reliable analytical methods are required to determine mycotoxins in foods and feeds. An improved QuEChERS extraction procedure was shown to be effective for simultaneous extraction of 12 mycotoxins from wheat, rice and maize flours.




Application NoteFood and Beverage

LC-MS/MS Analysis of Pesticide Residues in Rice and Unexpected Detection of Residues in an Organic Rice Sample

The use of pesticides in various stages of cultivation of basmati rice has increased in order to improve its production yield. A multi-residue pesticide method has been developed for the determination of pesticides in basmati rice. This application note shows the analysis of over 200 pesticides using a simple QuEChERS sample preparation procedure, followed by UltraPerformance LC® (UPLC®) couple to tandem quadrupole mass spectrometry.


Application NoteSeparations

Multi-Residue Pesticide Analysis in Dried Chili Powder: Optimized Cleanup after QuEChERS Extraction for UPLC-MS/MS and GC-MS/MS Analysis

This application note presents QuEChERS extraction and SPE-based cleanup strategies for multi-residue pesticide analysis of chili powder, a highly resinous and oily material obtained from dried chili pepper fruits. For the analysis of chili powder, the sample is first equilibrated with water before extraction using the DisQuE pouch for CEN QuEChERS.


Application NoteSeparations

A Validated Method for the Analysis of 142 Pesticide Residues Using Atmospheric Pressure GC Coupled with Tandem Quadrupole Mass Spectrometry

Various technologies are used to meet the challenge of multi-residue analysis of pesticides in food products destined for human consumption. This application note describes the development and validation of a multi-class method for the routine determination of 142 pesticide residues in various fruit and vegetable matrices.



Application NoteSeparations

QuEChERS Sample Preparation for the Determination of Polycyclic Hydrocarbons (PAH) in Shrimp Using LC with Fluorescence Detection

Major oil spills in the world’s oceans have brought attention to the problem of PAH contamination, and to the challenges related to PAH analysis in food and environmental samples. This application describes a QuEChERS-based sample preparation protocol for the determination of PAH in shrimp. QuEChERS methodology is quicker, easier, cheaper, safer than, and as rugged as prior methods of sample preparation.


Application NoteSeparations

QuEChERS Sample Preparation for LC/MS and LC/UV Determination of Carbendazin and Other Conazole Fungicides in Orange Juice

This application note discusses the sample preparation strategies for determination of conazole fungicides, including carbendazim, in orange juice. It is demonstrated that the DisQuE pouch (QuEChERS) from Waters is effective for extraction of conazole fungicides. The methodology described here provides high-throughput and low detection limits with a quick, simple, robust, and safe analysis. It is also shown that the QuEChERS extract can be readily utilized for UPLC/MS/MS analysis without further cleanup.

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