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Reliable Low-Level Analysis of Glycols in Water Using Split Injection

30 Jun 2019

Obtaining consistent results for low-level analysis of glycols in water samples is difficult when using splitless injection due primarily to issues with backflash, poor peak shape, and shifting retention times. The split injection method shown here avoids these problems and reliably produces good chromatographic results. Lifetime testing demonstrated that Rtx-Wax columns produce stable results, even after column integrity was challenged with 600 water injections.

Rtx-Wax Columns

Restek Corp.

Rtx-Wax columns are the most inert and efficient PEG columns currently available. The extended operating temperature range allows analysis of compounds having a wide volatility range and ensures low bleed at temperatures as high as 250 °C. Selectivity is comparable to other Carbowax columns for compounds of intermediate to high polarity.

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Reliable Low-Level Analysis of Glycols in Water Using Split Injection