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Waters TA Instruments ™ Coin Cell Differential Scanning Calorimeter

Evaluate coin cells’ thermal stability and decomposition without teardown

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TA Instruments - Waters LLC

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Description

Differential Scanning Calorimetry is a well-established technique to assess materials’ thermal properties, including phase transitions, onset temperature, and heat of reaction.

Complete Safety Testing of Fully Assembled Coin Cells

The Coin Cell DSC enables thermal assessment of coin cells, revealing energy release and reactions to inform safety and performance evaluation.

  • Direct coin cell testing of fully constructed 2032-coin cells without teardown
  • Quick, reliable thermal insights including onset temperature, reaction mechanism, heat of reaction, and off-gas analysis
  • Combine thermal and electrochemical signals for battery safety and performance testing
  • Complete safety characterization with both thermal and electrical signals from -80 to 600 °C

Advanced Features Engineered for Precise Thermal Diagnostics

Features:

  • Highly sensitive sensor enables more accurate onset temperature and heat flow measurement
  • Wide temperature range reveals battery behavior from –80 to 600 °C
  • Coin cell capsule maintains excellent contact with the sensor to cell failure
  • Evolved gas analysis compatible with MS, FTIR, or GC-MS to evaluate reaction mechanisms
  • Voltage monitoring supports state-of-charge and short circuit analysis

Fit-for-Purpose Battery Safety Testing

Battery developers can now verify new formulations’ safety in early-stage testing with less material and faster turnaround times than late-stage safety testing.

Dual Testing Modes

  • Scanning operating mode assesses thermal abuse, thermal degradation, onset temperature, heat of reaction and material cross-reaction
  • Isothermal operating mode evaluates heat flow during Solid Electrolyte Interface (SEI) formation, charge/discharge, overcharge, and overdischarge

Coin Cell Capsule

New coin cell capsules are compatible with 2032 and any 20 mm diameter coin cell. With its fit-for-purpose design, it suits testing of coin cells without teardown, providing accurate whole-cell safety testing previously impractical on a DSC.

  • Coin cell standard capsules maintain thermal signal throughout the full sample range
  • Coin cell cycling capsules optimize heat flow during isothermal cycling
  • 20 mm classic aluminum pans for material samples

Large Format DSC Cell Technology

The large format DSC cell’s exceptional reliability, accuracy, and reproducible heat flow measurements enable detection of even weak thermal transitions, revealing the early signs of battery degradation or failure. This reliability enables battery scientists to:

  • Assess battery material phase transitions
  • Identify reaction mechanisms
  • Improve battery safety by design

Complete Versatility in Battery Safety Testings

Interchangeable Cooling Systems

  • Finned Air Cooling System (FACS) for high temp heating from ambient to 600 °C
  • Refrigerated Cooling System (RCS) is capable of reaching –80 °C up to 400 °C

Evolved-Gas Analysis

EGA helps battery scientists understand reaction mechanisms and analyze off-gasses for safety. Compatible with:

  • Mass Spectrometry (MS)
  • Fourier Transform Infrared Spectroscopy (FTIR)
  • Gas Chromatography-Mass Spectrometry (GC-MS)

Electrochemical Connection

Combining thermal analysis, voltage monitoring, and cycling capabilities provides additional electrochemical insights including state-of-charge, internal short circuit and heat generated during cycling for safety and performance analysis. Users can connect the Coin Cell DSC to a:

  • Voltage monitoring device
  • Battery cycler
  • Potentiostat

Ultimate Data Control and Confidence

TRIOS™ Software is a state-of the art platform using cutting-edge technology for instrument control, data collection and data analysis for both rheology and thermal analysis.

  • Built-in coin cell testing templates
  • Intuitive and flexible data visualization
  • Automated analysis and report generation
  • Data export in JSON format for integration with LIMS
  • Unlimited licenses: access and analyze your data from anywhere

Specifications

Baseline Flatness≤500 μW
Baseline Repeatability ≤100 µW
Temperature Range[1]-80 °C to 600 °C
Temp Accuracy[2]±0.1 °C
Temp Precision[2]±0.05 °C
Enthalpy Precision[2]±1%
Heating Rate0.01 °C to 20 °C/min

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