Accurately Detect and Quantify 204 Pesticides of Global Food Safety Concern by LC-MS/MS

26 Apr 2017
Sarah Thomas
Associate Editor

Product news

Stop spending your time and money developing LC-MS/MS multi-residue pesticide methods and mixing reference standards when you could be running samples! Restek’s trusted food safety experts have already done the work for you—with guaranteed accuracy and at a lower cost.

Restek’s new certified reference materials (CRMs) for LC-MS/MS multi-residue pesticide analysis eliminate the need to source, purchase, and store individual materials along with the need to prepare your own mixes. Choose separate ampuls for mix-and-match customization or a complete kit that contains 204 compounds of interest, covering many LC-determined pesticides listed by government agencies. Designed for maximum shelf life, stability, and chromatographic performance, each standard ships with support documentation detailing Restek’s rigorous in-house quantitative testing. They even offer an optimized multi-residue pesticide method—including conditions and downloadable transition tables—free of charge.

Set up, verify, and validate your pesticide-screening methods in less time, with proven confidence, and at a significantly reduced cost by turning to Restek’s ISO-accredited labs for your LC-MS/MS multi-residue pesticide certified reference materials. For added convenience and unbeatable results, also consider their internal standards, Ultra and Pinnacle® DB LC columns, and Q-sep™ QuEChERS sample prep products.

LC Multi-Residue Pesticide Kit

Restek Corp.

Stop spending your time and money developing LC-MS/MS multi-residue pesticide methods and mixing reference standards when you could be running samples. Restek’s trusted food safety experts have already done the work for you—with guaranteed accuracy and at a lower cost.

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Q-sep™ QuEChERS Tubes

Restek Corp.

Q-sep™ QuEChERS Tubes for Pesticide Residue Analysis • Fast, simple sample extraction and cleanup using dSPE. • Fourfold increases in sample throughput. • Fourfold decreases in material cost. • Convenient, ready to use centrifuge tubes with ultra pure, preweighed adsorbent mixes. Quick, Easy, Cheap, Effective, Rugged, and Safe, the QuEChERS ("catchers") method, developed by the USDA Eastern Regional Research Center, has become very popular for extraction and clean-up of pesticide residue samples. Our products are available in three centrifuge tube sizes to meet the needs of both extraction and cleanup of a wide variety of sample matrices following various methods. The researchers developed a simple two-step procedure. First, the homogenized samples are extracted and partitioned, using an organic solvent and salt solution. Then, the supernatant is further extracted and cleaned, using a dispersive SPE technique. Multiple adsorbents are placed in a centrifuge tube, along with the 1mL of organic solvent and the extracted residues partitioned from step 1. The contents are thoroughly mixed, then centrifuged, producing a clean extract ready for a variety of GC or HPLC analytical techniques. Validation and proficiency data for the QuEChERS method are available for a wide variety of pesticides in several common food matrices on their website.

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LC-MSLC-MS (liquid chromatography-mass spectrometry) systems and equipment are used for separation and quantitative analysis of complex mixtures, combining liquid chromatography and mass spectrometry. Quantify proteins, contaminants, pesticides or screen for drug metabolites with a high level of sensitivity. LC-MS systems and equipment include reverse phase, normal phase and specialized columns integrated with various MS detectors such as time-of-flight (TOF), quadrupole, orbitrap or ion trap mass analyzers. LC-MS/MS instruments equipped with a qTOF or triple quadrupole analyzer give greater sensitivity and resolving power to your analysis. Find the best LC-MS equipment in our peer-reviewed product directory: compare products, check customer reviews and receive pricing direct from manufacturers.Environmental Monitoring and TestingEnvironmental monitoring and testing uses handheld portable analyzers, kits, spectrometers or chromatography systems for air, water, soil, food and other sample testing. Useful features of analyzers such as BOD and COD include portability, easy calibration, automation and sensitivity.  Environmental test kits for pH, water, moisture, etc, should be accurate, sensitive, reliable, fast and easy to use.QuEChERSThe QuEChERS (Quick, Easy, Cheap, Effective, Rugged, and Safe) method is a streamlined approach that is used to extract multi-residue target compounds from food samples. It is most commonly used by analytical chemists studying pesticide residues in food.PesticidesPesticides are used to protect crops from diseases, pests and unwanted plants. They are classed as persistent organic pollutants (POPs) and can be harmful to humans. The Environmental Protection Agency (EPA) currently regulates the use of pesticides in the USA. Food SafetyFood safety describes the prevention of food-borne illnesses. Contamination with a variety of pathogens can be prevented with adequate temperature control, hygiene and labeling. Food samples can be tested using GC/MS, HPLC, SPE, and qPCR to ensure their adherence to regulations.Food TestingFood testing refers to a variety experiments including PCR, mass spectrometry, processing, QuEChERS, analyzing and Kjeldahl.
Accurately Detect and Quantify 204 Pesticides of Global Food Safety Concern by LC-MS/MS