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Determination of Volatile Organic Compounds in Water-Based Paints and Varnishes Using GC-MS

29 Sept 2014

In this application note, a general GC-MS method was developed using the Shimadzu GC-MS-QP2010 Ultra, for the determination of 35 volatile organic compounds commonly found in water-based paints and varnishes.

GCMS-QP2010 Ultra Gas Chromatograph Mass Spectrometer

Capable of fast data measurement with sensitivity five times higher than previous models, the GCMS-QP2010 Ultra offers improved applicability for comprehensive two-dimensional GC and ultra-high separation. Shimadzu used new, patented mass spectrometry technology called Advanced Scanning Speed Protocol (ASSP™), a firmware protocol that optimizes the ion transmission hardware parameters with a highly efficient data collection algorithm, to increase data acquisition speed up to 20,000 u/sec and 100 Hz. ASSP also provides the added benefit of maintaining system sensitivity at elevated scan speeds. To help increase throughput, the GCMS-QP2010 Ultra features high-speed oven cooling for shorter analysis cycles. Using a double jet cooling system, the GC cools from 350 to 50 degrees Celsius in less than three minutes. The combination of a high-speed GC method and a high-speed cooling oven can reduce the analysis cycle by up to 50 percent. To further increase lab efficiency, the GCMS-QP2010 Ultra can accept two narrow-bore capillary columns into the MS simultaneously. Its twin-line MS system allows users to switch applications without physically modifying the column installation. Users simply decide which columns are required for analysis and choose the associated injection port.

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GC-MS GC-MS (gas chromatography-mass spectrometry) instruments and equipment are used to separate, quantify and identify mixtures of small and volatile compounds, such as polycyclic aromatics, fatty acids and alcohols. Often used in drug detection, forensic investigation and environmental analysis for pesticides and contaminants, GC-MS is a powerful addition to your lab’s analytical capabilities. GC-MS/MS instruments equipped with a qTOF or triple quadrupole analyzers can give greater sensitivity and resolution to your analysis. Find the best GC-MS instruments and equipment in our peer-reviewed product directory: compare products, check customer reviews and receive pricing direct from manufacturers.Volatile Organic Compounds (VOCs)Volatile organic compounds (VOCs) are chemicals that have a low boiling point. Some VOCs are harmful to human health, whereas others can be used to determine the shelf-life of foods samples. VolatilesVolatiles are a group of compounds that have a low boiling point and evaporate at room temperature. Volatiles, such as volatile organic compounds (VOCs), can be used to determine shelf-life of food samples. GC-MS is typically used to analyze volatiles.
Determination of Volatile Organic Compounds in Water-Based Paints and Varnishes Using GC-MS