Genevac Receives Positive Customer Commentary Regarding Rocket 4D

8 Oct 2013
Liam McNair
Administrator / Office Personnel

Genevac has reported very positive feedback from early adopters of their Rocket 4D – a fully automated system for automatic drying or concentration of very large volumes up to 100 liters.


Launched worldwide during the summer of 2013 – Genevac has received considerable interest, from laboratories drawn by the ease of use, automated productivity and performance of the Rocket 4D.

A chemistry scale-up laboratory at a major Pharma company, running kilo scale preparative Supercritical Fluid Chromatography (SFC), were drawn by the unattended automation offered by the Rocket 4D. Traditionally removing large volumes of methanol from their sample fractions using a number of rotary evaporators required a dedicated operator to top-up dry ice in cold traps, feed the systems with more product and watch the systems continually. The operator commented "With the Rocket 4D you simply load your sample, select a method, press start, and walk away – the system will do the rest. He added that he “got his life back” when the 4D arrived and now is able to spend his time much more productively.

A natural products research group, at a US Ivy League university, were faced with concentrating large volumes of aqueous extracts from vegetable tubers. Typical workflow for their chosen system for this new project would be for many scientists to have occasional access to the system. The university selected the Rocket 4D as it was easiest to operate, had technology to prevent sample bumping and did not require users to handle and clean large heavy glass evaporation vessels.

Compact in size the Rocket 4D allows you to dry or concentrate your samples with complete confidence as it uses proprietary vacuum technology to suppress solvent bumping and foaming – problems associated with sample loss when using large scale rotary evaporators.

The Rocket 4D comes as standard with a single, 5 liter 316 stainless steel vessel for drying or concentrating product. This has detachable handles and is easily lifted into and out of the evaporator. Access to the dried or concentrated product in the vessel is very easy. Dried products can be scooped out, or where enhanced user protection is needed, re-dissolved while the vessel is still in the system. Liquid products can be easily drained via a drain port in the side of the rotor, using a dedicated pouring stand Users wishing to dry volumes larger than five liters require the ‘Autofeed’ option, which enables the Rocket 4D to draw in product from the user’s own external supply. The Rocket 4D controls product feed, drying and the discharge of condensed waste solvent without any external intervention. The autofeed system has an integrated rinse circuit which enables dried products to be automatically re-dissolved in a small volume of solvent at the end of the process. Alternatively, the same circuit can be used under manual control for solvent exchange, by selecting a different solvent for re-dissolve. Cleaning the Rocket 4D between cycles is also very straightforward. The PTFE feed tubing is easily detached for cleaning or replacement and the vessel can be readily cleaned, wiped, inspected and even put in a dishwasher. The Rocket 4D also includes powerful cold traps that maximize solvent recovery protecting the environment and improving drying of samples.

Rocket 4D Synergy Large Volume Evaporator

Genevac

Rocket 4D Synergy is designed primarily to evaporate large sample volumes, with autofeed if required, allowing automatic evaporation of volumes up to 100 litres. Rocket 4D Synergy provides fast, safe evaporation for solvents with a boiling point of up to 165°C (DMF) and can easily dry aqueous samples. The system feeds the solution for evaporation to the evaporation vessel, controls temperature and pressure, prevents bumping and foaming, drains the condenser, stops when dry or concentrated, and if required, redissolves the product in a small volume of solvent, unattended, and with no user intervention. The Rocket 4D Synergy can also be fitted with a removable flask rotor to accommodate the full range of Rocket Sample handling solutions such as flasks, tubes and SampleGenie. Now you don't need to choose between flask or batch/feed evaporation. The Rocket and Rocket 4D Synergy evaporators will accommodate your process, whatever the volume. Each is capable of replacing several rotary evaporators and saving valuable bench space.

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