High Efficiency, Broad Scope Screening of Pesticides Using Gas Chromatography High Resolution Orbitrap Mass Spectrometry
10 Nov 2015Pesticides are used globally to improve the production and yields of agricultural crops and their use is essential to ensure a sufficient global food supply. However, this widespread use of pesticides and the potential for them to remain in the final product is of significant concern to consumers and to governments whose responsibility it is to ensure a safe food supply. Consequently, legislation exists to protect consumers from exposure to contaminated foods. This legislation requires that foods are monitored for both the type and quantity of the pesticide present, with each pesticide given a maximum residue limit (MRL) in a particular sample commodity. The list of compound and sample combinations is extensive, creating a challenge for accurate and reliable routine monitoring. This application notes evaluates the performance of the Thermo Scientific™ Q Exactive™ GC hybrid quadrupole-Orbitrap mass spectrometer (MS) for the accurate screening of GC-amenable pesticides.
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Thermo Scientific™ Q Exactive™ GC Orbitrap™ GC-MS/MS System
Thermo Fisher ScientificThe Thermo Scientific™ Q Exactive™ GC system is the first-ever combination of high resolution gas chromatography with high-resolution/accurate-mass (HR/AM) Orbitrap detection for the most comprehensive sample characterization. This easy-to-use system provides the most comprehensive characterization of samples in a single analysis for the highest confidence in compound discovery, identification, and quantitation. Building upon the flexible modularity of the Thermo Scientific™ TRACE™ 1300 Series GC, including user-exchangeable injectors and detectors, the Q Exactive GC system has the quantitative power of a GC triple quadrupole MS combined with the high precision, full scan high-resolution/accurate-mass capability that only Orbitrap technology can offer. Key Features: Advanced quadrupole technology (AQT) for high transmission of selected masses Resolving power up to 120,000 at m/z 200 Part-per-trillion-level sensitivity Thermo Scientific™ Extractabrite™ ion source for robust, rugged electron impact (EI) and chemical ionization (CI) performance Curved linear C-trap for precise ion injection HCD collision cell for higher energy collisional dissociation provides MS/MS ion characterization Intelligent identification software elucidates the nature of each injected sample. Applications: Untargeted and targeted metabolomics Food and beverage Industrial analyses Environmental Pharmaceutical Clinical and toxicology