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Quantification of Trace Crystal Polymorph Components using a High-speed 1-Dimensional Detector

Quantification of Trace Crystal Polymorph Components using a High-speed 1-Dimensional Detector

4 Jan 2016

Materials with the same chemical formula but different crystal structures are called polymorphs. Since an X-ray diffraction profile depends on the crystal structure of the measured materials, XRD is used to evaluate crystal polymorphs. In this application note, a trace component of anatase, a commercially sold reagent, was evaluated with a standard addition method by using a high-speed 1-dimensional detector.

UltimaIV

Rigaku Corporation

The Ultima IV represents the state-of-the-art in multipurpose X-ray diffraction (XRD) systems. Incorporating Rigaku's patented cross beam optics (CBO) technology for permanently mounted, permanently aligned and user-selectable parallel and focusing geometries, the Ultima IV X-ray diffractometer can perform many different measurements fast.With a multipurpose diffractometer, performance is measured by not only how fast you perform an experiment but also how fast you can switch between different types of experiments. Individual experiments are optimized with accessories like the D/teX Ultra high-speed position sensitive detector system, but the speed between experiments is radically improved with the combination of the automated alignment and CBO.The Ultima IV is the only XRD system on the market today that incorporates fully automatic alignment. When coupled with CBO and the in-plane arm, the automatic alignment capability makes the Ultima IV X-ray diffractometer the most flexible system available for multipurpose applications.UltimaIV Features: Full automated alignment under computer control. Optional in-plane diffraction arm for in-plane measurements without reconfiguration. Focusing and parallel beam geometries without reconfiguration. SAXS capabilities. Optional D/teX Ultra high-speed, position-sensitive detector system.

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SmartLab

Rigaku Corporation

The SmartLab is the most novel high-resolution diffractometer available today. Perhaps its most novel feature is the SmartLab Guidance software, which provides the user with an intelligent interface that guides you through the intricacies of each experiment. It is like having an expert standing by your side. The system incorporates a high resolution θ/θ closed loop goniometer drive system, cross beam optics (CBO), an in-plane scattering arm, and an optional 9.0 kW rotating anode generator.Coupling a computer controlled alignment system with a fully automated optical system and the Guidance software makes it easy to switch between hardware modes, ensuring that your hardware complexity is never holding back your research.Whether you are working with thin films, nanomaterials, powders, or liquids the SmartLab will give you the functionality to make the measurements you want to make when you want to make them.SmartLab Features: Full automated alignment under computer control. Optional in-plane diffraction arm for in-plane measurements without reconfiguration. Focusing and parallel beam geometries without reconfiguration. SAXS capabilities.

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MiniFlex Benchtop XRD

Rigaku Corporation

New 6th-generation general purpose benchtop XRD system for phase identification and phase quantification. New sixth generation MiniFlex X-ray diffractometer (XRD) is a multipurpose analytical instrument that can determine: phase identification and quantification, percent (%) crystallinity, crystallite size and strain, lattice parameter refinement, Rietveld refinement, and molecular structure. It is widely used in research, especially in material science and chemistry, as well as in industry for research and quality control. It is the newest addition to MiniFlex series of benchtop X-ray diffraction analyzers from Rigaku, which began with the introduction of the original MiniFlex system decades ago.   Overview: New 6th generation design Compact, fail-safe radiation enclosure Incident beam variable slit Simple installation and user training Factory aligned goniometer system Laptop computer operation Measurements: Phase identification Phase quantification Percent (%) crystallinity Crystallite size and strain Lattice parameter refinement Rietveld refinement Molecular structure Options: 8-position autosampler Graphite monochromator D/teX Ultra: silicon strip detector HyPix-400 MF: 2D HPAD detector Air sensitive sample holder Travel case

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Quantification of Trace Crystal Polymorph Components using a High-speed 1-Dimensional Detector